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绋卞彇2 g锛堢簿纰哄埌0.01 g锛夌殑鍧囧嫽妯ｅ搧浜�50 mL闆㈠績绠′腑锛屽姞鍏�8 mL涔欓吀閳夌珐娌栨恫锛屽厖鍒嗘贩鍕�锛屽啀鍔犲叆50 μL β-钁¤悇绯栭啗鑻烽叾 / 鑺冲熀纭吀閰叾锛屾贩鍕诲悗浜�37鈩冩按娴存按瑙�12 h銆傛坊鍔�100 μL 10 ng/mL鐨勫収(n猫i)妯�(bi膩o)娑蹭簬寰呮脯(c猫)妯ｅ搧涓�锛屽姞钃嬬疆浜庢按骞虫尟钑╁櫒涓尟钑�15 min锛�5000 r/min闆㈠績10 min銆傚彇4 mL涓婃竻娑插姞鍏�0.1 moL/L楂樻隘閰告憾娑�5 mL锛屾贩鍚堝潎鍕汇�傜敤楂樻隘閰歌(di脿o)绡�(ji茅)pH鍒�1±0.3銆�5000 r/min闆㈠績10 min鍚�锛屽皣鍏ㄩ儴涓婃竻娑诧紙绱�10 mL锛夎綁(zhu菐n)绉诲埌50 mL闆㈠績绠�锛岀敤10 moL/L鐨勬矮姘у寲閳夎(di脿o)绡�(ji茅)pH鍒�11銆傚姞鍏�10 mL椋藉拰姘寲閳夋憾娑插拰10 mL鐣颁笝閱�/涔欓吀涔欓叝锛�6:4锛夋贩鍚堟憾娑�锛屽厖鍒嗘彁鍙�锛屽湪5000 r/min闆㈠績10 min銆傝綁(zhu菐n)绉诲叏閮ㄦ湁姗�(j墨)鐩�锛屽湪40鈩冩按娴翠笅鐢ㄦ爱?d煤)鐛箞浼烇紲灏�? mL涔欓吀閳�锛岃秴鑱叉贩鍧囨憾瑙ｅ倷鐢�銆�
2.鍑堝寲锛�
灏囬櫧(y谩ng)闆㈠瓙浜ゆ彌灏忔煴閫ｆ帴鍒扮湡绌洪亷(gu貌)鏌辫缃�锛屽皣婧舵恫涓婃煴锛屼緷娆＄敤2 mL鍘婚洟瀛愭按銆�2 mL 2%鐢查吀姘存憾娑插拰2 mL鐢查唶娲楁粚鏌卞瓙骞跺竟搴曟娊骞�銆傛渶鍚庣敤2 mL鐨�5%姘ㄦ按鐢查唶婧舵恫娲楄劔鏌卞瓙涓婄殑寰呮脯(c猫)鎴愬垎銆傛祦閫熸帶鍒跺湪0.5 mL/min锛屾礂鑴恫鍦�40鈩冩按娴翠笅姘�?d煤)鐛箞浼烆棥?zh菙n)纰哄姞鍏�200 μL 0.1%鐢查吀/姘�-鐢查唶婧舵恫锛�95:5锛�锛岃秴鑱叉贩鍧�锛�15000 r/min闆㈠績10 min銆�
鈻� 妯�(bi膩o)婧�(zh菙n)鍝佸強鐩搁棞(gu膩n)瑭﹀姂
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鐢�(ch菐n)鍝佺法铏�(h脿o)
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鑻辨枃鍚嶇ū
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涓枃鍚嶇ū
|
CAS
|
鍖呰
|
|
|
Terbutalin sulfate
|
纭吀鍙斾竵瀵ф寜
|
|
0.1 g
|
|
|
Clenbuterol hydrochloride
|
楣介吀鍏嬩緰鐗圭緟
|
|
0.1 g
|
|
|
(±)-Clenbuterol D9 (trimethyl D9)
|
鍏嬪�壒缇�- D9
|
|
1 mL
|
|
|
Salbutamol free base
|
娌欎竵鑳洪唶
|
|
0.1 g
|
|
|
Salbutamol D3 (3-hydroxymethyl-D2,a D1)
|
娌欎竵鑳洪唶-D3
|
N/A
|
1 mL
|
|
|
Ractopamine hydrochloride
|
钀婂厠澶氬反鑳洪菇閰搁菇
|
|
0.1 g
|
|
|
Ractopamine-d6 Hydrochloride
|
钀婂厠澶氬反鑳�-d6
|
N/A
|
1 mg
|
|
|
β-Glucuronidase from Helix pomatia,β-D-Glucuronide glucuronosohydrolase
|
BETA-钁¤悇绯栭啗閰哥敊閰�
|
|
1 MU
|
|
|
Tulobuterol
|
濡ュ竷鐗圭緟
|
|
100 mg
|
|
|
Fenoterol hydrobromide
|
姘捍閰搁潪璜剧壒缇�/閰氫笝鍠樺鑺繏閱�
|
|
1 mL
|
|
|
Formoterol Fumarate Dihydrate
|
绂忚帿鐗圭緟瀵岄Μ閰搁菇浜屾按鍚堢墿
|
|
25 mg
|
|
|
Isoxsuprine hydrochloride
|
N/A
|
N/A
|
1 EA
|
|
|
Cimaterol
|
N/A
|
N/A
|
50 mg
|
|
|
Clenbuterol-D9 hydrochloride
|
N/A
|
N/A
|
25 mg
|
|
|
Salbutamol free base
|
娌欎竵鑳洪唶
|
|
1 mL
|
|
|
Terbutaline-d9
|
5-(1-缇ュ熀-2-鍙斾竵鍩烘皑鍩轰箼鍩�)鑻�-1,3-浜岄厷
|
N/A
|
1 mg
|
|
|
Cimbuterol
|
N/A
|
N/A
|
50 mg
|
|
|
Brombuterol hydrochloride
|
N/A
|
N/A
|
50 mg
|
|
|
Mabuterol hydrochloride
|
棣竷鐗规礇楣介吀楣�
|
|
50 mg
|
|
|
Mapenterol hydrochloride
|
N/A
|
|
50 mg
|
|
|
Bromchlorbuterol hydrochloride
|
N/A
|
N/A
|
50 mg
|
|
|
Methanol, 99.9% [HPLC/ACS]
|
鐢查唶
|
|
4 L
|
|
|
2-Propanol, 99.8%[HPLC/ACS]
|
鐣颁笝閱�
|
|
4 L
|
|
|
Ethyl acetate, 99.9% [HPLC/ACS]
|
涔欓吀涔欓叝
|
|
4 L
|
|
|
Formic acid, for analysis, 99+%
|
鐢查吀
|
|
1 L
|
|
|
Ammonium hydroxide, 28-30 wt% solution of NH3 in water, for analysis
|
姘ㄦ按
|
|
1 L
|
|
|
Acetic acid, sodium salt, anhydrous, for analysis, 99+%
|
涔欓吀閳�
|
|
250 g
|
鈻� 閰嶅鍎�鍣ㄨ�楁潗
|
鐢�(ch菐n)鍝佺法铏�(h脿o)
|
鐢�(ch菐n)鍝佸悕绋�
|
鍖呰
|
|
|
鍔犵啽纾佸姏鏀媽鍣�
|
1 鑷�(t谩i)
|
|
|
RCT 鍩烘湰鍨嬬鍔涙敧鎷屽櫒
|
1 鑷�(t谩i)
|
|
|
纾佸姏鏀媽瀛�
|
1 PK
|
|
|
鎵嬪嫊(d貌ng)鍠亾鍙(di脿o)寮忕Щ娑叉锛�1000-5000 µL
|
1 鏀�
|
|
|
鐡跺彛鍒嗘恫鍣�锛�5-50 mL
|
1 鍊�(g猫)
|
|
|
8247 R95 鏈夋(j墨)钂告埃鐣板懗闃茶(h霉)鍙ｇ僵锛�120鍊�(g猫)/绠�
|
1 绠�
|
|
|
SCX Polymer - Box, 50 x 3 mL tubes, 60 mg
|
50 鏀�/鐩�
|
|
|
Eclipse Plus C18, 2.1 x 50 mm,1.8 µm, 600 bar
|
1 鏀�
|
|
|
100 mL, DURAN, NS 14/23, -stoer
|
1 濂�
|
|
|
Screw cap vials, clear 100/PK 閫忔槑铻哄彛2 mL妯ｅ搧鐡�
|
1 鐩�
|
|
|
寰瓟婵捐啘肖50 0.2 μ锛堟按锛夋贩鍚堢簴缍礌
|
100 鐗�/鍖�
|
|
|
寰瓟婵捐啘肖50 0.2 μ锛堟湁姗�(j墨)锛夊凹榫�
|
100 鐗�/鍖�
|
|
|
婧跺姂閬�(gu貌)婵惧櫒(1 L) 鏉�300 mL 鐡�1000 mL锛孭TFE婵炬澘
|
1 濂�
|
|
|
12 Port Vacuum Extraction Manifold Assy
|
1 濂�
|