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      闅ㄨ憲钘ョ墿鍚堟垚闋�(l菒ng)鍩熺殑鐧�(f膩)灞�锛�“鐞嗘兂鐨�”鍚堟垚鏂规硶鎴愮偤浜嗘柊鐨勭櫦(f膩)灞曢噸榛�(di菐n)锛�鍗冲挤(qi谩ng)瑾�(di脿o)瀵�(sh铆)鐢�銆佺挵(hu谩n)澧冨弸濂�銆佽硣婧愬彲鎸佺簩(x霉)鍒╃敤锛�寰炵啊(ji菐n)鍠槗寰楃殑鍘熸枡鍑虹櫦(f膩)锛�鍦ㄦ韩鍜岀殑姊濅欢涓嬬稉(j墨ng)閬庣啊(ji菐n)鍠殑姝ラ锛�蹇�熴�侀珮閬告搰鎬у湴杞�(zhu菐n)鍖栫偤鐩(bi膩o)鍒嗗瓙銆傜稜鑹插寲瀛�(xu茅)鏄暥(d膩ng)鍓嶅寲瀛�(xu茅)瀛�(xu茅)绉戠櫦(f膩)灞曠殑涓昏鏂瑰悜锛屽埄鐢ㄧ稜鑹插悎鎴愬伐钘濆埗鍌欒棩鐗�锛屽彲鎻愰珮鍘熷瓙鍒╃敤鐜�锛岄檷浣庡虎妫勭墿鐨勭敘(ch菐n)鐢�锛屽悓鏅�(sh铆)娓涜紩钘ョ墿鍚堟垚灏�(du矛)鐠�(hu谩n)澧冨拰浜洪珨鐨勫奖闊�[1]銆�

      鐧鹃潏濞佸緸鍋ュ悍瀹夊叏锛岀挵(hu谩n)澧冨弸濂界瓑鍥犵礌鍑虹櫦(f膩)锛岀偤绉戠爺宸ヤ綔鑰呭�戠攧閬镐簡涓�绯诲垪鐨�“缍犺壊瑭﹀姂”銆�

鍦�1.鍒╃敤缍犺壊瑭﹀姂MMPP锛�566277锛�鍦ㄥ婧笅鍚堟垚纭掗叜鍖栧悎鐗�[2]

References

[1] 闄冲▉榫�. 缍犺壊鍖栧(xu茅)鍦ㄨ棩鐗╁悎鎴愪腑鐨勬噳(y墨ng)鐢╗J]. 涓皬浼佹キ(y猫)绠＄悊鑸囩鎶�鏃垔, 2016(3): 275-275.

[2] Temperini A, Curini M, Rosati O, et al. Magnesium bis (monoperoxyphthalate) hexahydrate as mild and efficient oxidant for the synthesis of selenones[J]. Beilstein journal of organic chemistry, 2014, 10(1): 1267-1271.

 

 

鈻� 缍犺壊鍚堟垚瑭﹀姂

 

鐢�(ch菐n)鍝佺法铏�(h脿o)

鐢�(ch菐n)鍝佸悕绋�

CAS

绲�(ji茅)妲�(g貌u)寮�

鍖呰

180331

N,N'-Carbonyldiimidazole, 98%

N,N'-缇板熀浜屽挭鍞� 98%

 530-62-1

5 G

25 G

100 G

500 G

260292

2-Chloro-4,6-dimethoxy-1,3,5-triazine, 97%

2-姘�-4,6-浜岀敳姘у熀-1,3,5-涓夊棯 97%

 3140-73-6

1 G

5 G

25 G

100 G

102492

2-Chloro-1-methylpyridinium iodide 97%

2-姘�-1-鐢插熀鍚″暥閹撶鍖栫墿 97%

 14338-32-0

5 G

25 G

100 G

199549

N-Chlorosuccinimide, 97.5%

N-姘唬鐞ョ弨閰颁簽鑳� 97.5%

 128-09-6

25 G

100 G

500 G

275928

N,N'-Dicyclohexylcarbodiimide, 99%

N,N'-浜岀挵(hu谩n)宸卞熀纰充簩浜炶兒 99%

538-75-0

25 G

100 G

250 G

1 KG

211112

N-(3-Dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride, 99%

N-(3-浜岀敳姘ㄥ熀涓欏熀)-N'-涔欏熀纰充簩浜炶兒楣介吀楣� 99%

25952-53-8

1 G

10 G

50 G

100 G

250 G

207005

N-Ethoxycarbonyl-2-ethoxy-1,2-dihydroquinoline, 99%

N-涔欐哀?锛�?span lang="EN-US">-2-涔欐哀鍩�-1,2-浜屾矮鍠瑰晧 99%

 16357-59-8

5 G

25 G

100 G

566277

 

Monoperoxyphthalic acid magnesium salt hexahydrate 70%

鍠亷姘ч劙鑻簩鐢查吀閹傞菇鍏按鍚堢墿 70%

84665-66-7

 

25 G

100 G

500 G

293019

N,N,N',N'-Tetramethylfluoroformamidinium hexafluorophosphate,97%

N,N,N’,N’-鍥涚敳鍩烘盁浠ｈ劜閹撳叚姘熺７閰搁叝 97%

164298-23-1

1 G

5 G
 
鈻�鏇村鐢�(ch菐n)鍝佽珛(q菒ng)瑕嬶細

 鐧鹃潏濞佺稜鑹插寲瀛�(xu茅)-鏈夋(j墨)灏忓垎瀛愬偓鍖栧姂

鐧鹃潏濞侀洟瀛愭恫楂�—鐛�(d煤)鐗规�ц兘鐨勭稜鑹叉憾鍔�

J&K璨撮噾灞偓鍖栧姂&閰嶉珨

钘ョ墿涓殑鍎�(y艒u)鍕�(sh矛)绲�(ji茅)妲�(g貌u)—鍚�N椋藉拰闆滅挵(hu谩n)鍖栧悎鐗�

鏂板瀷涓嶅皪(du矛)绋卞悎鎴愬偓鍖栧姂&閰嶉珨—鎵嬫�ф爱姘у寲鍚堢墿

 

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